Xylem MULTI 3400 MULTI-PARAMETER METERS Bedienungsanleitung Seite 1

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ba75688e01 01/2007
Multi 3400i
Operating manual
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ARng
TP
pH/Dissolved Oxygen/Conductivity
Measuring Instrument
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Inhaltsverzeichnis

Seite 1 - Multi 3400i

ba75688e01 01/2007Multi 3400iOperating manualARRCLSTOCALMO671927O°Cmg/lARngTPpH/Dissolved Oxygen/ConductivityMeasuring Instrument

Seite 2 - © Weilheim 2007, WTW GmbH

Overview Multi 3400i101.6 Operating structureThe following overview diagram shows which keys you have to press to select between the different measuri

Seite 3 - Multi 3400i List of contents

Multi 3400i Safety112 SafetyThis operating manual contains basic instructions that you must follow during the commissioning, operation and maintenance

Seite 4 - List of contents Multi 3400i

Safety Multi 3400i122.2 General safety instructionsThis instrument is built and inspected according to the relevant guide-lines and norms for electron

Seite 5 - 1Overview

Multi 3400i Commissioning133 Commissioning3.1 Scope of deliveryz Multi 3400i handheld meter z Plug-in power supply unitz Operating manual and short op

Seite 6 - 1.2 SETs of equipment

Commissioning Multi 3400i14Connecting theplug-in power supplyYou can either operate the measuring instrument with batteries or with the plug-in power

Seite 7 - Multi 3400i Overview

Multi 3400i Operation154 Operation4.1 Switching on the measuring instrumentMeasuring mode whenswitching onNote The measuring instrument has an energy

Seite 8 - 1.3 Keypad

Operation Multi 3400i164.2 pH value / ORP voltage4.2.1 General informationPreparatory activities Perform the following preparatory activities when you

Seite 9 - UpH SalO

Multi 3400i Operation17Temperature measure-ment in pH measure-mentsYou can perform pH measurements with or without a temperature sen-sor as well as wi

Seite 10 - 1.6 Operating structure

Operation Multi 3400i184.2.2 Measuring the pH valueAutoRead AR(Drift control)The AutoRead function (drift control) checks the stability of the mea-sur

Seite 11 - ECHNICAL DATA must

Multi 3400i Operation19NoteThe current AutoRead measurement can be terminated at any time (accepting the current value) by pressing <RUN/ENTER>.

Seite 12 - ECHNICAL DATA

Accuracy whengoing to pressThe use of advanced technology and the high quality standard of our instruments are the result of continuous development. T

Seite 13 - 3.1 Scope of delivery

Operation Multi 3400i204.2.4 pH calibrationWhy calibrate? pH electrodes age. This changes the asymmetry (zero point) and slope of the pH electrode. As

Seite 14 - Commissioning Multi 3400i

Multi 3400i Operation21Sample printout: Calibration evaluation After calibrating, the measuring instrument automatically evaluates the calibration. Th

Seite 15 - 4 Operation

Operation Multi 3400i22Preparatory activitiesAutoCal TEC For this procedure, use any two WTW technical buffer solutions (pH values at 25 °C: 2.00 / 4.

Seite 16 - 4.2 pH value / ORP voltage

Multi 3400i Operation23NoteAt this point, the AutoCal TEC calibration can be terminated with <M>. This corresponds to a single-point calibration

Seite 17 - Multi 3400i Operation

Operation Multi 3400i246 Thoroughly rinse the electrode with distilled water.7 If required, enter the temperature of the first buffer solution, while

Seite 18 - Operation Multi 3400i

Multi 3400i Operation2512 Switch to the measuring mode with <M>.YAS0RCLSalcmAutoCal DINTimeDay.MonthSalStoreAR8No.IdentTref20Tref25YearBaudcmC/%

Seite 19

Operation Multi 3400i264.3 Dissolved oxygen4.3.1 General informationNoteD. O. measurements with the Multi 3400i can only be carried out using a CellOx

Seite 20 - INTERFACE, page 51)

Multi 3400i Operation274.3.2 Measuring the D. O. concentrationWhen measuring the concentration of test samples with a salt content of more than 1 g/l,

Seite 21 - HAT TO DO IF

Operation Multi 3400i284.3.3 Measuring the D. O. saturationYou can measure the D. O. saturation as follows: 4 While pressing the <RUN/ENTER> key

Seite 22

Multi 3400i Operation294.3.4 AutoRead AR (Drift control)The AutoRead function (drift control) checks the stability of the mea-surement signal. The sta

Seite 23 - OO UpHUpH SalSal

Multi 3400i List of contents31 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51.1 General features . . . . . .

Seite 24

Operation Multi 3400i304.3.5 D. O. calibrationWhy calibrate? D. O. probes age. This changes the slope of the D. O. probe. Calibra-tion determines the

Seite 25

Multi 3400i Operation31Probe evaluation After the calibration, the measuring instrument evaluates the current status of the probe against the relative

Seite 26 - 4.3 Dissolved oxygen

Operation Multi 3400i32NoteIn chapter 6 WHAT TO DO IF... page 65, you will find the measures to take for error elimination.5 Press the <RUN/ENTER&g

Seite 27

Multi 3400i Operation334.3.6 Salt content correctionA salt content correction is required in the oxygen concentration mea-surement of samples with a s

Seite 28

Operation Multi 3400i344.4 Conductivity4.4.1 General informationNoteConductivity measurements with the Multi 3400i can only be carried out using the T

Seite 29

Multi 3400i Operation35Checking thecell constant1 Press the <RCL> key repeatedly until CAL disp appears on the display. 2 Press the <RUN/ENT

Seite 30

Operation Multi 3400i364.4.2 Measuring the conductivityYou can carry out the conductivity measurements as follows:4.4.3 Measuring the salinityYou can

Seite 31

Multi 3400i Operation374.4.4 AutoRead AR (Drift control)The AutoRead function (drift control) checks the stability of the mea-surement signal. The sta

Seite 32

Operation Multi 3400i384.4.5 Determining the cell constant (Calibration in the control standard)Why determine the cellconstant?Aging slightly changes

Seite 33 - EASURING THE SALINITY

Multi 3400i Operation39Calibration evaluation After the calibration, the measuring instrument automatically evaluates the current status of the calibr

Seite 34 - TURE, page 58

List of contents Multi 3400i44.7.2 PC/external printer (RS232 interface) . . . . . . . . 554.7.3 Remote control . . . . . . . . . . . . . . . . . .

Seite 35 - IN THE CONTROL STANDARD)

Operation Multi 3400i40NoteIf the error message E3E3E3E3 appears, refer to chapter 6 WHAT TO DO IF...5 To return to the measuring mode: Press the <

Seite 36

Multi 3400i Operation414.5 Calibration intervals (Int 3, Int 4, Int 5)For each measured variable, a time interval is stored. When it has ex-pired, you

Seite 37

Operation Multi 3400i424.6 Saving dataThe Multi 3400i portable measuring instrument has an internal data memory. It can store up to 500 datasets. A co

Seite 38

Multi 3400i Operation43Message StoFullStoFullStoFullStoFull This message appears when all of the 500 storage locations are occu-pied.You have the foll

Seite 39

Operation Multi 3400i444.6.2 Switching on AutoStore (Int 1)The save interval (Int 1) determines the chronological interval between automatic save pro

Seite 40

Multi 3400i Operation45As soon as all of the 500 storage locations are occupied, AutoStore is terminated (Int 1 = OFF). If there are not enough storag

Seite 41

Operation Multi 3400i464.6.3 Outputting the data storageYou can output the contents of the data storage:z Stored data on the displayz Calibration data

Seite 42 - 4.6 Saving data

Multi 3400i Operation47NoteIf you want to search for a certain element of the data record (e.g. date), proceed as follows:Outputting stored datato the

Seite 43 - StoFullStoFull

Operation Multi 3400i48Sample printout:Outputting the calibra-tion dataon the display No. 1: 09.03.01 17:10pH 10.01 25 °CTauto

Seite 44

Multi 3400i Operation492 Press the <RUN/ENTER> key. The data of the last calibration of all measured variables ap-pears in the following sequenc

Seite 45

Multi 3400i Overview51Overview1.1 General featuresThe compact precision handheld meter Multi 3400i enables you to car-ry out pH measurements, dissolve

Seite 46

Operation Multi 3400i505 Press <RUN/ENTER> to display the cell constant. The dis-played value is:z the current, calibrated cell constant (with s

Seite 47

Multi 3400i Operation51Outputting the calibra-tion protocol on theinterfaceSample printout:1 Press the <RCL> key repeatedly until CAL SEr appear

Seite 48

Operation Multi 3400i524.6.4 Clearing the memoryWith this function, you can delete the stored data records. 500 storage locations will then be availab

Seite 49

Multi 3400i Operation534.7 Transmitting dataYou have the following possibilities of transmitting data:z One of the following options:– With the AutoSt

Seite 50

Operation Multi 3400i54NoteWhen the AutoStore function is active at the same time, the data trans-mission is performed according to the setting of the

Seite 51

Multi 3400i Operation554.7.2 PC/external printer (RS232 interface)Via the RS 232 interface, you can transmit the data to a PC or an ex-ternal printer.

Seite 52

Operation Multi 3400i564.8 ConfigurationYou can adapt the handheld meter to your individual requirements. To do this, the following parameters can be

Seite 53 - 4.7 Transmitting data

Multi 3400i Operation57Displaying theair pressureThe air pressure is only displayed if an oxygen sensor is connected. Otherwise, "---" appea

Seite 54

Operation Multi 3400i58Dissolved oxygencalibration intervalConductivitycalibration intervalSwitching over thereference temperature10 Confirm with <

Seite 55 - 3 Ground

Multi 3400i Operation59Date and time15 Using <▲> <▼>, toggle between t20 and t25.16 Confirm with <RUN/ENTER>. The date flashes on th

Seite 56 - 4.8 Configuration

Overview Multi 3400i61.2 SETs of equipmentThe measuring instrument is also available as part of individual SETs of equipment. You will find additional

Seite 57

Operation Multi 3400i604.9 Reset You can reset (initialize) the measurement parameters and the config-uration parameters separately from one another.M

Seite 58

Multi 3400i Operation61Resetting themeasuring parameters1 Press the <RUN/ENTER> key and hold it down.2 Press the <CAL> key. The setting to

Seite 59

Operation Multi 3400i62Resetting theconfiguration parame-ters7 Using <▲ > <▼>, switch between no and YES.YES: Resetting the Cond measuring

Seite 60 - 4.9 Reset

Multi 3400i Maintenance, cleaning, disposal635 Maintenance, cleaning, disposal5.1 MaintenanceThe measuring instrument is almost maintenance-free. The

Seite 61

Maintenance, cleaning, disposal Multi 3400i64NoteFor maintenance of electrodes, probes and measuring cells refer to the relevant operating manuals.5.2

Seite 62

Multi 3400i What to do if...656 What to do if...6.1 pH system messagesError message 0FL0FL0FL0FL Error message E3E3E3E3 Cause RemedypH electrode:– N

Seite 63 - 5.1 Maintenance

What to do if... Multi 3400i66 No stable measuredvalue Obviously incorrectmeasured valuesBuffer solutions– Incorrect buffer solutions – Change calib

Seite 64 - 5.3 Disposal

Multi 3400i What to do if...676.2 Oxi system messagesError message 0FL0FL0FL0FLError message E3E3E3E3Error message E7E7E7E7AR flashescontinuously Caus

Seite 65 - 6.1 pH system messages

What to do if... Multi 3400i68Measured value too lowMeasured value toohigh6.3 Conductivity system messagesError message OFLOFLOFLOFL Error message E3

Seite 66 - What to do if... Multi 3400i

Multi 3400i What to do if...696.4 General errorsDisplay LoBat Instrument does notreactto keystroke Display totototo Probe symbol flashes Message Sto

Seite 67 - 6.2 Oxi system messages

Multi 3400i Overview77 50 ml pH buffer solution, STP 48 50 ml pH buffer solution, STP 79 Calibration and control standard for conductivity measuring c

Seite 68

What to do if... Multi 3400i70

Seite 69 - AINTENANCE)

Multi 3400i Technical data717 Technical dataDimensions and weightMechanical structure Electrical safety Ambient conditions pH/ORP measuringranges Pre

Seite 70

Technical data Multi 3400i72Oxi measuring rangesMeasuring range/resolu-tion temperaturePrecision ofOxi (± 1 digit) Correction functions ofOxi Cond mea

Seite 71 - 7 Technical data

Multi 3400i Technical data73Precision ofCond (± 1 digit) Cell constant,calibrating Cond referencetemperature Serial interface Connection of the cable

Seite 72 - Technical data Multi 3400i

Technical data Multi 3400i74Power supply Guidelinesand norms used Batteries 4 x 1.5 V alkali-manganese batteries, Type AAOperational life Approx. 300

Seite 73 - Multi 3400i Technical data

Multi 3400i Technical data75Test certificates FCC Class A Equipment StatementNote: This equipment has been tested and found to comply with the limits

Seite 74

Technical data Multi 3400i76

Seite 75

Multi 3400i Lists778ListsThis chapter provides additional information and orientation aids.Abbreviations The list of abbreviations explains the indica

Seite 76

Lists Multi 3400i78AbbreviationsConductivity value (international γ)AR AutoRead (drift control)ARng Automatic range switchingMeasuring instrument meas

Seite 77 - Multi 3400i Lists

Multi 3400i Lists79nLF Nonlinear temperature compensationOFL Display range exceeded (Overflow)OxiCal Automatic calibration for D. O. measurementspH p

Seite 78

Overview Multi 3400i81.3 KeypadKey functionsRUN/ENTERARRCLCALSTOMSelect the measured variable <M>:– pH value / ORP voltage– D. O. concentration

Seite 79

Lists Multi 3400i80GlossaryAdjusting To manipulate a measuring system so that the relevant value (e. g. the displayed value) differs as little as poss

Seite 80 - Lists Multi 3400i

Multi 3400i Lists81Measuring system The measuring system comprises all the devices used for measuring, e. g. measuring instrument and probe. In addit

Seite 81

Lists Multi 3400i82Salt content General designation for the quantity of salt dissolved in water.Sample Designation of the sample ready to be measured.

Seite 82

Multi 3400i Index83IndexAAir pressure display 57Asymmetry 20Authorized use 11AutoCal TEC 20, 22AutoRange (oxygen) 15AutoReadConductivity 37D. O. 29pH

Seite 83 - Multi 3400i Index

Index Multi 3400i84values 53Two-point calibration (pH) 20, 23

Seite 84 - Two-point calibration (pH)

Wissenschaftlich-Technische Werkstätten GmbHDr.-Karl-Slevogt-Straße 1D-82362 WeilheimGermanyTel: +49 (0) 881 183-0+49 (0) 881 183-100Fax: +49 (0) 881

Seite 85

Multi 3400i Overview91.4 Display1.5 Jack field1 D. O. probe or conductivity measuring cell2 pH electrode 3 pH temperature sensor4 Plug-in power supply

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